GC-søjler

cyclodextrin derivatives with high melting point:
for GC-enantiomer separation diluted with polysiloxanes
Heptakis-(2,3-di-O-methyl-6-O-t-butyldimethyl-silyl)-β-cyclodextrin. Phase diluted with optimised polysiloxane recommended for γ-lactones, cyclopentanones, terpenes, esters, tartrates.

• Max. temperature for isothermal operation: 230°C
• Max. temperature for short isotherms in a temperature programme: 250°C

cyclodextrin derivatives with high melting point:
for GC-enantiomer separation diluted with polysiloxanes
Heptakis-(2,3-di-O-acetyl-6-O-t-butyldimethyl-silyl)-β-cyclodextrin. Phase diluted with optimised polysiloxane recommended for alcohols, esters, ketones, aldehydes, δ-lactones.

• Max. temperature for isothermal operation: 220°C
• Max. temperature for short isotherms in a temperature programme: 240°C

LIPODEX^® cyclodextrin phase for enantiomer separation

base material: cyclic oligosaccharide consisting of eight glucose units bonded through α-1,4-linkages (y-cylodextrin) regioselective alkylation and acylation of the hydroxyl groups leads to a lipophilic phase, which is well suited for GC enantiomer analyses; important advantage: many compounds can be analysed without derivatisation (however, for certain substances enantioselectivity can be favourably influenced by formation of derivatives)

LIPODEX^® E is suitable for a broad application range.
Octakis-(2,6-di-O-pentyl-3-O-butyryl)-γ-cyclodextrin. Recommended for α-amino acids, α- and β-hydroxycarboxylic acid esters, alcohols (TFA), diols (TFA), ketones, pheromones (cyclic acetals), amines, alkyl halides, lactones.

• Max. temperature for isothermal operation: 200°C
• Max. temperature for short isotherms in a temperature programme: 220°C

70% Cyanopropyl Polysilphenylene-siloxane. Able to be solvent rinsed. Industry standard column for fatty acid methyl esters, carbonhydrates, pharmaceuticals, GC/MS applications. Suitable alternative to: DB-23, Rtx-2330, SP-2330, CP-Sil 88, SP2380, HP-23.

5% Phenyl Polysilphenylene-siloxane. General purpose GC column for routine gas chromatographic analysis. Suitable replacement for: DB-5, DB-5ms, DB-5.625, XTI-5, Rtx-5ms, Ultra-2, HP-5, HP-5MS, HP5-TA, SPB-5, MDN-5S, CP-Sil8CB, Rxt-Sil 5MS, AT-5ms, VB-5, ZB-5, VF-5ms.

• Very low bleed
• Non-polar
• Extremely inert

5% Phenyl Polycarborane siloxane. Ultra-high temperature columns for simulated distillation applications, general hydrocarbon profiles, pesticides, herbicides and for GCMS applications.

8 % Phenyl Polycarborane-siloxane. Ultra high temperature columns for polychlorinated biphenyl compounds (PCB), nitro-substituted aromatics, polynuclear aromatic hydrocarbons, pesticides and herbicides.

Polyethylene Glycol (PEG) in a SolGel matrix. Suitable replacement for: DB-Wax, Rtx- Wax, Stabilwax, HP20M, HP-Wax, HP-INNOWax, Supelcowax-10, AT-Wax, Nukol, CP, Wax 52CB, VB-WAX, ZB-WAX.

• Robust high-temperature column.
• Polar phase
• Low bleed and inert

100% dimethylpolysiloxane

nonpolar phase separation of components according to boiling points thick film columns ≥3µm film are especially recommended for solvent analysis.
Similar phases: Permabond^® SE-30, OV-1, DB-1, SE-30, HP-1, SPB-1, CP-Sil 5 CB, Rtx-1, 007-1, BP1, MDN-1, AT-1, ZB-1, OV-101.
For columns with 0.25 to 0.32mm ID and films <3µm the max. temperature for isothermal operation is 340°C, the max. temperature for short isotherms in a temperature programme is 360°C.
For 0.53mm ID columns with films <3µm the max. temperatures are 320 and 340°C, resp. for thick film columns with films ≥3µm the max. temperatures are 300 and 320 °C, resp.

100 % dimethylpolysiloxane

nonpolar phase with ultra-low bleeding, ideal for ion trap and quadrupol MS detectors increased sensitivity due to an unmatched low background level perfect inertness for basic compounds
solvent rinsing for removal of impurities applicable
application areas: all-round phase for environmental analyses, trace analyses, EPA methods, pesticides, PCB, food and drug analyses
similar phases: Ultra-1, DB-1 MS, HP-1 MS, Rtx-1 MS, Equity™1, AT-1 MS, VF-1 MS, CP-Sil 5 CB MS
max. temperature for isothermal operation 340 °C, max. temperature for short isotherms in a temperature programme 360 °C

phenylmethylpolysiloxane (50 % phenyl)

medium polar phase
preferred applications: steroids, pesticides, drug analyses
USP G3
similar phases: OV-17, DB-17, HP50+, HP17, SPB-50, SP-2250, Rtx-50, CP-Sil 24 CB, 007-17, ZB50

max. temperature for isothermal operation: 320°C, max. temperature for short isotherms in a temperature programme: 340°C, for 0.53mm ID columns the max. temperatures are 300 and 320°C, resp.

14 % Cyanopropyl-phenyl - 86 % Dimethylpolysiloxane

USP G46
medium polar phase
special selectivity due to high cyanopropyl content
reference column for structure identification, e.g. in combination with Optima 5
film thickness 1 µm for solvent analyses
similar phases: OV-1701, DB-1701, CP?Sil 19 CB, HP-1701, Rtx-1701, SPB-1701, 007-1701, BP10, ZB-1701

max. temperature for isothermal operation: 300°C, max. temperature for short isotherms in a temperature programme: 320°C
for 0.53mm ID columns the max. temperatures are 280 and 300°C, resp.

50% cyanopropylmethyl - 50% phenylmethylpolysiloxane

USP G7 / G19
middle polar phase
recommended for fatty acid analyses
similar phases: DB-225, HP-225, OV-225, Rtx-225, CP-Sil 43, 007-225, BP225

max. temperature for isothermal operation: 260°C, max. temperature for short isotherms in a temperature programme: 280°C

especially deactivated for the analysis of polyfunctional amines such as ethanolamines, amino-functionalised diols and similar compounds, which are important base materials in industrial chemistry, and shows strong tailing on standard-deactivated columns; similar phases: Rtx-5 Amine, PTA-5; USP G27 / G36; improved linearity for analyses of active components at trace levels: no amine absorptions even for aliphatic and aromatic amines at concentrations of 100 pg/peak; tested with the Optima^® Amine test mixture, which among others also contains diethanolamine and propanol-pyridine (this test mixture is supplied with each column). Max. temperature for isothermal operation: 300°C, max. temperature for short isotherms in a temperature programme: 320°C.

5% phenyl - 95% dimethylpolysiloxane

USP G27, G36 nonpaolar standard phase with large range of application similar phases: Permabond^® SE-52 , SE-54, SE-52, DB-5, HP-5, SPB-5, CP-Sil 8, Rtx-5, 007-5, BP5, MDN-5, AT-5, ZB-5 for columns with 0.1 to 0.32mm ID and films <3µm the max. temperature for isothermal operation is 340°C, the max. temperature for short isotherms in a temperature programme is 360°C for 0.53mm ID columns with films < 3µm the max. temperatures are 320 and 340°C, resp. for thick film columns with films ≥ 3µm the max. temperatures are 300 and 320°C, resp.

Further lengths available on request.

silarylene phase

• With polarity similar to a 5 % diphenyl -95 % dimethylpolysiloxane phase.
• USP G27, G36
• Lowest column bleed, nonpolar phase, ideal for ion trap and quadrupol MS detectors solvent rinsing for removal of impurities applicable
• Application areas: all-round phase for environmental analyses, trace analyses, EPA methods, pesticides, PCB, food and drug analyses

5% diphenyl - 95% dimethylpolysiloxane

nonpolar phase with low bleeding, deal for GC/MS and ECD applications and general analyses at trace level perfect inertness for basic compounds.
Similar phases: DB-5 MS, HP-5 MS, Ultra-2, Equity-5, CP-Sil 8 CB low bleed/MS, Rtx-5SIL-MS, Rtx-5 MS, 007-5 MS, BPX5, MDN-5S, AT-5 MS, VF-5 MS.
max. temperature for isothermal operation: 340°C, max. temperature for short isotherms in a temperature programme: 360 °C

6% cyanopropyl-phenyl - 94% dimethylpolysiloxane

USP G43
medium polar phase
recommended for environmental analyses
similar phases: HP-624, HP-VOC, DB-624, DB-VRX, SPB-624, CP-624, Rtx-624, Rtx-Volatiles, 007-624, BP624, VOCOL

max. temperature for isothermal operation: 280°C, max. temperature for short isotherms in a temperature programme: 300°C

6% cyanopropyl-phenyl - 94% dimethylpolysiloxane

USP G 43
medium polar phase
low bleed columns for halogenated hydrocarbons, volatiles, aromatic compounds, solvents etc.
similar phases: HP-624, HP-VOC, DB-624, DB-VRX, SPB-624, CP-624, Rtx-624, Rtx-Volatiles, 007-624, BP624, VOCOL

max. temperature for isothermal operation: 280°C, max. temperature for short isotherms in a temperature programme: 300°C

polyethylene glycol 2-nitroterephthalate

close equivalent USP G25 / G35
polar phase
recommended for FAME, free carboxylic acids
similar phases: Permabond FFAP , DB-FFAP, HP-FFAP, CP-Sil 58 CB, 007-FFAP, CP-FFAP CB, Nukol

for columns with 0.10 to 0.32mm ID the max. temperature for isothermal operation is 250°C, the max. temperature for short isotherms in a temperature programme is 260°C for 0.53mm ID columns the max. temperatures are 220 and 240°C, resp.

polyethylene glycol 20000 daltons

USP G16
polar phase
recommended for solvent analysis and alcohols
suitable for aqueous solutions
similar phases: Premabond^® CW 20 M , DB-Wax, Supelcowax, HP-Wax, HP-INNOWAX, Rtx-Wax, CP-Wax 52 CB, Stabilwax, 007-CW, BP20, AT-Wax, ZB-Wax

Max. temperature for isothermal operation 240°C, max. temperature for short isotherms in a temperature programme: 250°C,
for 0.53 mm ID columns the max. temperatures are 220 and 240°C, resp.

100% Dimethyl Polysiloxane. General purpose GC column for all routine analyses such as hydrocarbons, aromatics, pesticides, phenol, herbicides and amines. Suitable replacement for: DB-1, DB-Petro, HP-1, HP-1MS, Rtx-1, Ultra-1, SPB-1, SPB-1 Sulfur, Petrocol DH, CP-Sil 5CB, VB-1, ZB-1, VF-1ms.

• Low bleed
• Non-polar

Polyethylene Glycol phase. GC column for analyses such as alcohol, free acids, fatty acid methyl esters, aromatics, solvents and essential oils. Suitable replacement for: Carbowax 20M, CP-Wax 52 CB, DB-WAX, Elite-WAX, HP-20M, HP-INNOWax RH-WAX, Rtx-Wax, Stabilwax, SUPELCOWAX 10, TG-WaxMS, VF-WAXms, ZB-WAX.

• Industry standard wax column
• Polar phase

Nitroterephtalic acid modified PEG. For low molecular weight acids, alcohols, aldehydes, acrylates and ketones. Suitable replacement for: DB-FFAP, HP-FFAP, Stabilwax-DA, CPWax-58CB.

• Polar phase
• Able to be solvent rinsed (water or methanol are not recommended for rinsing)

5% Phenyl / 95% Dimethyl Polysiloxane. Low bleed. General purpose GC column for all routine analyses such as aromatics, pesticides, herbicides, hydrocarbons. Suitable replacement for: DB-5, Rtx-5, HP-5, Ultra-2, PTE-5, SPB-5, MDN-5, CP-Sil 8CB, VB-5, ZB-5, VF-5ms.

5% Phenyl Polysilphenylene-siloxane. For 5% GC-MS analysis and general purpose MS analysis. Suitable replacement for: DB-5ms, ZB-5ms, Rxi-5Sil MS, VF-5ms, CP-Sil 8 CB.

Cyanopropylphenyl Polysiloxane. For the analysis of volatile components of drinking water, chlorinated hydrocarbons, solvents and for the EPA method 624, USP G43 methods, SW-846 and 8240 / 8260 methods. Suitable replacement for: DB-624, OV-624, AT-624, HP-VOC, CP-Select624CB, 007-624, Rtx-Volatiles, VOCOL, ZB-624.

Cyanopropyl Polysilphenylene. Polar phase. For environmental analyses, volatile organic substances, alcohol analyses and for the EPA method 624, USP G43 methods, 502.2, SW-846 and 8240 / 8260 methods. Suitable replacement for: DB-VRX, HP-624, OPTIMA 624, ELITE-624, 007-624, RTXVOLATILES, SPB-624, TRV1, CPSIL 13 CB, VOCOL, VB-624, CP-624.

100% Dimethyl Polysiloxane. For high temperature hydrocarbon analysis and ASTM methods D2887 and D6532. Suitable replacement for: DB-2887, DB-HT Sim Dis, HP-1, Petrocol 2887, Petrocol EX2887, Rtx-2887.

• Non-polar
• Low bleed

35 % Phenyl Polysilphenylene-siloxane. Suitable Replacement for: DB-35, DB-35ms, Rtx-35, HP-35, HP-35MS, SPB-35, MDN-35.

• Very low bleed
• Inert
• Mid polarity column
• Equivalent to USP phase G42
• High temperature
• Able to be solvent rinsed

90% Cyanopropyl Polysilphenylene-siloxane. For the fast separation of fragrances, aromatics, pesticides, PCB, isomers of fatty acid methyl esters.

• Bonded phase
• Highly polar
• Thermally stable
• Able to be solvent rinsed

100% Dimethyl Polysiloxane. For the analysis of petroleum products. Suitable Replacement for: Petrocol DH, DB-Petro, HP-PONA, AT-Petro, Elite-PONA, ZB-1, 007-1-100-0.5F, Rtx-1PONA, CP Sil PONA.

• Non-polar phase for PONA analysis
• Detailed hydrocarbon analysis according to ASTM
• Crosslinked and washable
• Very high resolving power columns for complex samples

14 % Cyanopropylphenyl Polysiloxane. For analysis of organochlorine pesticides. Suitable replacement for: DB-1701, Rtx-1701, SPB-7, HP-1701, CP-Sil 19CB, 007-1701, PE-1701, SP-1701.

• Low bleed
• Highly inert
• Able to be solvent rinsed

For Dioxins and related compounds (POPs, PCBs, PCDFs, PCDDs).

• Very low bleed
• Non-polar
• Extremely inert
• Ideal for GC-MS

50% Phenyl Polysilphenylene-siloxane. For a range of EPA methods (604, 608, 8060, 8081), pharmaceutical applications, triazines, herbicides and steroids. Suitable replacement for: OV-17, SP-2250, DB-17, DB-17ms, DB-17ht, Rtx-50, SPB-50, HP-50+, HP-17.

35% Phenyl Polysilphenylene-siloxane. For environmental analyses, EPA 608, pesticides and herbicides. Suitable replacement for: DB-608, Rtx-35, SPB-608, HP-35, ZB-35.

Permethylated Beta-Cyclodextrin (Chiral). Suitable replacement for: Cyclodex-B, Rt-BDEXm, LIPODEX C. Phase for the separation of chiral compound e.g. separation of enantiomeric compounds found in natural products.

100% Dimethyl Polysiloxane in a SolGel matrix. Suitable Replacement for: DB-1, DB-Petro, HP-1, HP-1MS, Rtx-1, Ultra-1, SPB-1, SPB-1 Sulfur, Petrocol DH, CP-Sil 5CB, VB-1, ZB-1, VF-1ms.

• Less bleed
• Non-polar
• Highly inert
• Same selectivity as BP1

Liners come individually packed complete with instrument appropriate o-rings and sealing rings. Each pack is supplied with quality test results. Further liners und pack sizes available on request.